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BS ISO 22682:2017

$142.49

Iron ores. Determination of trace elements. Plasma spectrometric method

Published By Publication Date Number of Pages
BSI 2017 32
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This document specifies a method for the determination of phosphorus, vanadium, titanium, copper, nickel, chromium, barium and cobalt in iron ores, by inductively coupled plasma atomic emission spectrometry (ICP-AES).

This method is applicable to the concentration ranges (mass fraction) given in Table 1, in natural iron ores, iron ore concentrates and agglomerates, including sinter products.

Table 1

Concentration ranges

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 1 Scope
2 Normative references
8 3 Terms and definitions
4 Principle
5 Reagents
10 6 Apparatus
7 Sampling and samples
7.1 Laboratory sample
11 7.2 Preparation of predried test samples
8 Procedure
8.1 Number of determinations
8.2 Test portion
8.3 Blank test and check test
8.4 Determination
8.4.1 Decomposition of the test portion
12 8.4.2 Adjustment of spectrometer
13 9 Calculation of results
9.1 Calibration graph
14 9.2 Correction of spectral interference
15 9.3 Standardization of calibration graph (drift correction)
16 9.4 General treatment of results
9.4.1 Repeatability and permissible tolerances
9.4.2 Determination of analytical result
17 9.4.3 Check for trueness
18 9.4.4 Calculation of final result
9.5 Oxide factors
10 Test report
20 Annex A (informative) Suggested calibration solutions
21 Annex B (normative) Plasma spectrometer performance tests
24 Annex C (normative) Flowchart of the procedure for the acceptance of analytical values of test samples
25 Annex D (informative) Derivation of repeatability and permissible tolerance formulae
26 Annex E (informative) Precision data obtained by international analytical trials
31 Bibliography
BS ISO 22682:2017
$142.49