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ASTM-D3828 2009

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D3828-09 Standard Test Methods for Flash Point by Small Scale Closed Cup Tester

Published By Publication Date Number of Pages
ASTM 2009 9
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ASTM D3828-09

Historical Standard: Standard Test Methods for Flash Point by Small Scale Closed Cup Tester

ASTM D3828

Scope

1.1 These test methods cover procedures for flash point tests, within the range of 30 to 300°C, of petroleum products and biodiesel liquid fuels, using a small scale closed cup tester. The procedures may be used to determine, whether a product will or will not flash at a specified temperature (flash/no flash Method A) or the flash point of a sample (Method B). When used in conjunction with an electronic thermal flash detector, these test methods are also suitable for flash point tests on biodiesels such as fatty acid methyl esters (FAME).

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.3 WarningMercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPAs website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.

1.4 This standard should be used to measure and describe the properties of materials, products, or assemblies in response to heat and flame under controlled laboratory conditions and should not be used to describe or appraise the fire hazard or fire risk of materials, products, or assemblies under actual fire conditions. However, results of this test may be used as elements of a fire risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard of a particular end use.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Warning statements appear throughout. See also the Material Safety Data Sheets for the product being tested.

Keywords

combustible; fire risk; flammable; flash point; volatile; Calibration–petroleum analysis instrumentation; Flash/no flash method; Flash point–liquids; Setaflash testers; Volatility–petroleum products

ICS Code

ICS Number Code 75.100 (Lubricants, industrial oils and related products)

DOI: 10.1520/D3828-09

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
2 Terminology
Summary of Test Methods
Significance and Use
Apparatus
Reagents and Materials
Sampling
3 Preparation of Apparatus
Verification of Apparatus
Procedure
4 Procedure
Calculation
TABLE 1
5 Report
Precision and Bias
Keywords
A1. FLASH TEST APPARATUS
A1.1 Flash Test Apparatus
A1.2 Test Cup
A1.3 Test Flame and Pilot Flame
TABLE 2
6 FIG. A1.1
7 A1.4 Audible Signal
A1.5 Syringe
A1.6 Syringe
A1.7 Flash Detector (optional)
A1.8 Timing Device
A1.9 Temperature Measuring Device
A1.10 Electric Ignitor Screen
A2. VERIFICATION OF APPARATUS PERFORMANCE
A2.1 Certified Reference Material (CRM)
TABLE A1.1
TABLE A2.1
8 A2.2 Secondary Working Standard (SWS)
A3. PRECISION FOR FATTY ACID METHYL ESTERS (FAME)
A3.1 Background
A3.2 Equivalence
A3.3 Precision and Bias10
A4. SUB-AMBIENT TESTING FOR MANUAL APPARATUS WITHOUT INTEGRAL TEST CUP COOLING FACILITIES
A4.1 Apparatus Using a Liquid in Glass Thermometer
A4.2
A4.3
A4.4
ASTM-D3828 2009
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