ASTM-D4322 2001
$40.63
D4322-96(2001)e1 Standard Test Method for Residual Acrylonitrile Monomer Styrene-Acrylonitrile Copolymers and Nitrile Rubber by Headspace Gas Chromatography (Withdrawn 2010)
| Published By | Publication Date | Number of Pages |
| ASTM | 2001 | 8 |
ASTM D4322-96-e1-Reapproved2001
Withdrawn Standard: Standard Test Method for Residual Acrylonitrile Monomer Styrene-Acrylonitrile Copolymers and Nitrile Rubber by Headspace Gas Chromatography (Withdrawn 2010)
ASTM D4322
Scope
1.1 This test method is suitable for determining the residual acrylonitrile (RAN) content of styrene-acrylonitrile (SAN) copolymer, rubber-modified acrylonitrile-butadiene-styrene (ABS) resins, and nitrile rubber (NBR).
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.
Note 1–Although the packed column option of this test method and ISO 4581:1994 (E) differ in some details, data obtained using either test method should be technically equivalent. There is no equivalent ISO standard for the capillary column option of this test method.
Keywords
headspace gas chromatography; nitrile rubber; residual acrylonitrile; styrene-acrylonitrile copolymers
ICS Code
ICS Number Code 83.060 (Rubber)
DOI: 10.1520/D4322-96R01E01
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 1 | Scope Referenced Documents Terminology Summary of Test Method Significance and Use |
| 2 | Interferences Apparatus Reagents and Materials |
| 3 | Safety Precautions Sampling and Storage Preparation of Gas Chromatograph for Packed Column Analysis FIG. 1 |
| 4 | Preparation of Gas Chromatograph for Capillary Column Analysis Calibration by Standard Addition for Packed Column Analysis |
| 5 | Calibration with an Internal Standard for Packed Column Analysis Calibration with an External Standard for Capillary Column Analysis FIG. 2 |
| 6 | Manual Sample Analysis Procedure for Packed Column Analysis Automated Sample Analysis Procedure for Packed Column Analysis Automated Sample Analysis Procedure for Capillary Column Analysis Calculations—Standard Addition Method for Packed Column Analysis Calculations—Internal Standard Method for Packed Column Analysis Calculation—External Standard Method for Capillary Column Analysis |
| 7 | Precision and Bias FIG. 3 TABLE 1 TABLE 2 |
| 8 | Keywords |
