ASTM-D5317:2011 Edition

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D5317-98(2011) Standard Test Method for Determination of Chlorinated Organic Acid Compounds in Water by Gas Chromatography with an Electron Capture Detector

Published By	Publication Date	Number of Pages
ASTM	2011	15

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Categories: 71.080.40 - Organic acids, ASTM

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Description

ASTM D5317-98-Reapproved2011

Historical Standard: Standard Test Method for Determination of Chlorinated Organic Acid Compounds in Water by Gas Chromatography with an Electron Capture Detector

ASTM D5317

Scope

1.1 This test method covers a gas chromatographic procedure for the quantitative determination of selected chlorinated acids and other acidic herbicides in water. Similar chemicals may also be determined by this test method, but it is the user’s responsibility to verify the applicability of this test method to any compounds not listed in this scope. The acid form of the following compounds were interlaboratory tested using this test method, and the results were found acceptable:

Keywords

electron capture; gas chromatography; herbicides; organic acid; Chlorinated phenoxy acid herbicide; Electron-capture detectors (ECD); Gas chromatography (GC)–water; Herbicides; Organic acid; Total free acid

ICS Code

ICS Number Code 71.080.40 (Organic acids)

DOI: 10.1520/D5317-98R11

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents
2	Terminology Summary of Test Method Significance and Use Interferences
3	Apparatus and Equipment FIG. 1 TABLE 1
4	Reagents and Materials
5	Hazards Sample Collection, Preservation, and Storage Calibration
6	Procedure
8	Esterification Magnesium Silicate Separation Extract Storage Chromatography FIG. 2
9	Calculation Precision and Bias
10	TABLE 2
11	Quality Control TABLE 3
12	TABLE 4 TABLE 5
14	Keywords X1. Example Calculation Of Acceptance Criteria for Initial Demonstration Of Proficiency X1.1 Maximum Acceptable Standard Deviation (Sm) X1.2 Acceptance Range for Mean Recovery
15	REFERENCES

Additional information

Standard Title	D5317-98(2011) Standard Test Method for Determination of Chlorinated Organic Acid Compounds in Water by Gas Chromatography with an Electron Capture Detector
Published Code	ASTM
Publication Date	2011
Pages Count	15
ICS Codes	71.080.40 - Organic acids