ASTM-D86 2011

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D86-11b Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure

Published By	Publication Date	Number of Pages
ASTM	2011	11

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Category: ASTM

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Description

1.1 This test method covers the atmospheric distillation of petroleum products using a laboratory batch distillation unit to determine quantitatively the boiling range characteristics of such products as light and middle distillates, automotive spark-ignition engine fuels with or without oxygenates (see Note 1), aviation gasolines, aviation turbine fuels, diesel fuels, biodiesel blends up to 20 %, marine fuels, special petroleum spirits, naphthas, white spirits, kerosines, and Grades 1 and 2 burner fuels.

Note 1An interlaboratory study was conducted in 2008 involving 11 different laboratories submitting 15 data sets and 15 different samples of ethanol-fuel blends containing 25 v%, 50 v%, and 75 v% ethanol. The results indicate that the repeatability limits of these samples are comparable or within the published repeatability of the method (with the exception of FBP of 75% ethanol-fuel blends). On this basis, it can be concluded that Test Method D86 is applicable to ethanol-fuel blends such as Ed75 and Ed85 (Specification D5798 ) or other ethanol-fuel blends with greater than 10 v% ethanol. See ASTM RR:D02-1694 for supporting data.

1.2 The test method is designed for the analysis of distillate fuels; it is not applicable to products containing appreciable quantities of residual material.

1.3 This test method covers both manual and automated instruments.

1.4 Unless otherwise noted, the values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.

1.5 WARNING Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA s website http://www.epa.gov/mercury/faq.htm for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents
2	Terminology Summary of Test Method
3	Significance and Use Apparatus FIG. 1
4	FIG. 2
5	Sampling, Storage, and Sample Conditioning FIG. 3 FIG. 4 FIG. 5 TABLE 1
6	Preparation of Apparatus TABLE 2
7	Calibration and Standardization Procedure TABLE 3
8	TABLE 4
9	FIG. 6 TABLE 5
11	Calculations TABLE 6
12	Report
13	Precision and Bias Keywords
14	A1. PRECISION TABLES FOR REPEATABILITY (r) AND REPRODUCIBILITY (R) A1.1 Tables
15	A2. DETAILED DESCRIPTION OF APPARATUS A2.1 Distillation Flasks A2.2 Condenser and Condenser Bath A2.3 Metal Shield or Enclosure for Flask A2.4 Heat Source A2.5 Flask Support
16	A2.6 Flask Support Board A2.7 A2.8 A2.9 Receiving Cylinders A2.10 Residue Cylinder FIG. A2.1
17	FIG. A2.2
18	FIG. A2.3 FIG. A2.4
19	A3. DETERMINATION OF THE DIFFERENCE IN LAG TIME BETWEEN AN ELECTRONIC TEMPERATURE MEASUREMENT SYSTEM AND A MERCURY-IN-GLASS THERMOMETER A3.1 A3.2 A3.3 A3.4 A3.5 A3.6 A4. PROCEDURE TO DETERMINE THE PERCENT EVAPORATED OR PERCENT RECOVERED AT A PRESCRIBED TEMPERATURE READING A4.1 A4.2 A4.3 A4.4 A4.5 Manual Distillation A4.6 Automated Distillation
20	A4.7 Calculations A4.8 Precision A4.9 A4.10 TABLE A4.1
21	TABLE A4.2 TABLE A4.3 TABLE A4.4 TABLE A4.5
22	X1. EXAMPLES ILLUSTRATING CALCULATIONS FOR REPORTING OF DATA X1.1 X1.2 Temperature Readings at Prescribed Percent Evaporated X2. EXAMPLES OF CALCULATION OF REPEATABILITY AND REPRODUCIBILITY OF VOLUME % (RECOVERED OR EVAPORATED) AT A PRESCRIBED TEMPERATURE READING X2.1 X2.2 Example Calculation FIG. X1.1
23	X3. TABLES OF CORRECTED LOSS FROM MEASURED LOSS AND BAROMETRIC PRESSURE X3.1 X3.2 TABLE X2.1 FIG. X3.1
24	X4. PROCEDURE TO EMULATE THE EMERGENT STEM ERROR OF A MERCURY-IN-GLASS THERMOMETER X4.1 X4.2 X4.3 X5. EXPLANATORY REPORT FORMS X5.1 FIG. X3.2
25	FIG. X5.1
26	FIG. X5.2

Additional information

Standard Title	D86-11b Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure
Published Code	ASTM
Publication Date	2011
Pages Count	11

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