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ASTM-E2330 2004

$40.63

E2330-04 Standard Test Method for Determination of Trace Elements in Glass Samples Using Inductively Coupled Plasma Mass Spectrometry (ICP-MS)

Published By Publication Date Number of Pages
ASTM 2004 6
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1.1 This test method covers a procedure for elemental analysis of magnesium (Mg), aluminum (Al, titanium (Ti), manganese (Mn), gallium (Ga), rubidium (Rb), strontium (Sr), zirconium (Zr), antimony (Sb), barium (Ba), lanthanum (La), cerium (Ce), samarium (Sm), hafnium (Hf) and lead (Pb) in the bulk of glass samples (irregularly shaped and as small as 200 micrograms) for the comparison of fragments of a known source to the recovered fragments from a questioned source. These elements are present in soda lime and borosilicate glass in ngg -1 to % levels. Alternative methods for the determination of elemental analysis of glass are listed in the references. This procedure may also be applicable to other elements, other types of glass, or other concentration ranges with appropriate modifications of the digestion procedure (if needed for full recovery of the additional elements) and the mass spectrometer conditions. The addition of calcium and potassium, for example, could be added to the list of analytes in a modified analysis scheme.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Summary of Test Method
Significance and Use
Apparatus
2 Calibration
Procedure
Precision and Bias
Keywords
3 X1. ISOTOPES
X1.1 Trace Elements
X1.2 High Standards
TABLE X1.1
TABLE X1.2
TABLE X1.3
4 X2. LIMITS
X3. BIAS AND PRECISION
TABLE X2.1
TABLE X3.1
5 REFERENCES
TABLE X3.2
TABLE X3.3
TABLE X3.4
ASTM-E2330 2004
$40.63