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ASTM-E975 2008

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E975-03(2008) Standard Practice for X-Ray Determination of Retained Austenite in Steel with Near Random Crystallographic Orientation

Published By Publication Date Number of Pages
ASTM 2008 7
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ASTM E975-03-Reapproved2008

Historical Standard: Standard Practice for X-Ray Determination of Retained Austenite in Steel with Near Random Crystallographic Orientation

ASTM E975

Scope

1.1 This practice covers the determination of retained austenite phase in steel using integrated intensities (area under peak above background) of X-ray diffraction peaks using chromium KĪ± or molybdenum KĪ± X-radiation.

1.2 The method applies to carbon and alloy steels with near random crystallographic orientations of both ferrite and austenite phases.

1.3 This practice is valid for retained austenite contents from 1 % by volume and above.

1.4 If possible, X-ray diffraction peak interference from other crystalline phases such as carbides should be eliminated from the ferrite and austenite peak intensities.

1.5 Substantial alloy contents in steel cause some change in peak intensities which have not been considered in this method. Application of this method to steels with total alloy contents exceeding 15 weight % should be done with care. If necessary, the users can calculate the theoretical correction factors to account for changes in volume of the unit cells for austenite and ferrite resulting from variations in chemical composition.

1.6 Unitsā€”The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

austenite; crystallographic orientation; ferrite; martensite; retained austenite; X-ray diffraction; Austenite (retained); Austenitic steel; Crystallographic characteristics; Ferritic steel; HSLA (high-strength low-alloy) steel; Martensitic steel; Random crystallographic orientation; Retained austenite; Structural metals/alloys; X-ray diffraction analysis

ICS Code

ICS Number Code 77.080.20 (Steels)

DOI: 10.1520/E0975-03R08

PDF Catalog

PDF Pages PDF Title
1 Scope
Significance and Use
2 Principles for Retained Austenite Measurement by X-Ray Diffraction
TABLE 1
3 Procedure
4 FIG. 1
5 TABLE 2
6 Example
Precision and Bias
Report
Keywords
TABLE 3
ASTM-E975 2008
$40.63