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BS EN 17864:2023

$102.76

Inorganic fertilizers. Determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea)

Published By Publication Date Number of Pages
BSI 2023 16
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This document specifies a method for the determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea) using high-performance liquid chromatography (HPLC). The method is applicable to all fertilizers which do not contain interfering organic compounds.

PDF Catalog

PDF Pages PDF Title
2 undefined
5 European foreword
6 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus and equipment
7 7 Sampling and sample preparation
8 Procedure
8.1 General
8.2 Calibration
8.2.1 Stock solution IBDU, mass concentration ρ(IBDU) = 100 mg/l
8.2.2 Stock solution CDU, ρ(CDU) = 100 mg/l
8.2.3 Calibration solutions
8 Table 1 — Preparation of calibration solutions
8.3 Preparation of the test solution
8.4 Measurement
9 Calculation and expression of the result
9 10 Precision
10.1 Inter-laboratory tests
10.2 Repeatability
10.3 Reproducibility
Table 2 — Mean values, repeatability and reproducibility limits
11 Test report
10 Annex A (informative) Results of the inter-laboratory tests
Table A.1 — Statistical results of the inter-laboratory tests
11 Annex B (informative) Example chromatogram and calibration curves
B.1 Example chromatogram
Figure B.1 — Example chromatogram
B.2 Example calibration curves
12 Figure B.2 — Example calibration curve CDU
Figure B.3 — Example calibration curve IBDU
13 Annex C (informative) Example conditions for a suitable HPLC system
14 Bibliography
BS EN 17864:2023
$102.76