BS EN 17864:2023
$102.76
Inorganic fertilizers. Determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea)
Published By | Publication Date | Number of Pages |
BSI | 2023 | 16 |
This document specifies a method for the determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea) using high-performance liquid chromatography (HPLC). The method is applicable to all fertilizers which do not contain interfering organic compounds.
PDF Catalog
PDF Pages | PDF Title |
---|---|
2 | undefined |
5 | European foreword |
6 | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 5 Reagents 6 Apparatus and equipment |
7 | 7 Sampling and sample preparation 8 Procedure 8.1 General 8.2 Calibration 8.2.1 Stock solution IBDU, mass concentration ρ(IBDU) = 100 mg/l 8.2.2 Stock solution CDU, ρ(CDU) = 100 mg/l 8.2.3 Calibration solutions |
8 | Table 1 — Preparation of calibration solutions 8.3 Preparation of the test solution 8.4 Measurement 9 Calculation and expression of the result |
9 | 10 Precision 10.1 Inter-laboratory tests 10.2 Repeatability 10.3 Reproducibility Table 2 — Mean values, repeatability and reproducibility limits 11 Test report |
10 | Annex A (informative) Results of the inter-laboratory tests Table A.1 — Statistical results of the inter-laboratory tests |
11 | Annex B (informative) Example chromatogram and calibration curves B.1 Example chromatogram Figure B.1 — Example chromatogram B.2 Example calibration curves |
12 | Figure B.2 — Example calibration curve CDU Figure B.3 — Example calibration curve IBDU |
13 | Annex C (informative) Example conditions for a suitable HPLC system |
14 | Bibliography |