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BS EN ISO 16181-1:2021

BS EN ISO 16181-1:2021

$142.49

Footwear. Critical substances potentially present in footwear and footwear components – Determination of phthalate with solvent extraction

Published By Publication Date Number of Pages
BSI 2021 24
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This document specifies a test method to determine the qualitative and quantitative presence of phthalate compounds (see Annex A) in footwear and footwear components.

NOTE 1

A list of relevant materials potentially containing phthalates can be found in ISO/TR 16178:2012, Annex A or in CEN/TR 16417 .

NOTE 2

This test method can also be used to determine phthalates other than those listed in Annex A, subject to validation.

PDF Catalog

PDF Pages PDF Title
2 National foreword
4 European foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
8 5 Reagents
5.1 Chemicals
5.1.2 Internal standard
5.2 Standard solutions
5.2.1 Target phthalates — Stock solution
5.2.2 Internal standard — Stock solution
9 5.2.3 Calibration solutions
5.2.4 Extraction solution with internal standard (optional)
6 Apparatus
10 7 Sampling
8 Test procedure
8.1 Extraction
8.1.1 Ultrasonic extraction
8.1.2 Alternative extraction procedure for PVC materials
11 8.1.3 Preparation of a method blank
8.2 Determination with GC-MS
9 Expression of results
9.1 Calibration curve
9.2 Determination of the phthalates content
9.2.1 For each phthalate
12 9.2.2 When a sum of phthalates is requested
9.3 Performance of the test method
10 Test report
13 Annex A (informative) Information on some identified phthalates
14 Annex B (informative) Information on some identified phthalates
16 Annex C (informative) Suitable gas chromatography-mass spectrometry (GC-MS) apparatus and detection limits for determination of phthalates
18 Annex D (informative) Results of the interlaboratories tests – Method using toluene extraction (8.1.1)
20 Annex E (informative) Example of a chromatogram for selected phthalates
21 Annex F (informative) Comparison of extraction of phthalates by using toluene and THF
23 Bibliography

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BS EN ISO 16181-1:2021
$142.49