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BS ISO 10810:2010

$167.15

Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis

Published By Publication Date Number of Pages
BSI 2010 38
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PDF Catalog

PDF Pages PDF Title
9 1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
10 5 Overview of sample analysis
5 Overview of sample analysis
12 6 Specimen characterization
6.1 General
6.2 Specimen forms
6.2.1 General
6 Specimen characterization
6.1 General
6.2 Specimen forms
6.2.1 General
13 6.2.2 Single crystal
6.2.3 Adsorbed or segregated layers, films and residues
6.2.4 Interfaces and multilayered samples
6.2.5 Non-porous
6.2.6 Porous
6.2.7 Powder
6.2.8 Fibres and textiles
6.2.9 Internal interface
6.2.2 Single crystal
6.2.3 Adsorbed or segregated layers, films and residues
6.2.4 Interfaces and multilayered samples
6.2.5 Non-porous
6.2.6 Porous
6.2.7 Powder
6.2.8 Fibres and textiles
6.2.9 Internal interface
14 6.3 Material types
6.3.1 General
6.3.2 Metals and alloys
6.3.3 Polymers
6.3.4 Semiconductors
6.3.5 Magnetic materials
6.3.6 Ceramics
6.3.7 Catalysts
6.3.8 Glass and insulators
6.3.9 Biological
6.3 Material types
6.3.1 General
6.3.2 Metals and alloys
6.3.3 Polymers
6.3.4 Semiconductors
6.3.5 Magnetic materials
6.3.6 Ceramics
6.3.7 Catalysts
6.3.8 Glass and insulators
6.3.9 Biological
15 6.4 Handling and mounting of specimens
6.5 Specimen treatments
6.5.1 General
6.5.2 Heating and cooling
6.5.3 Scraping and fracture
6.5.4 Ion bombardment for analysing thin films
6.5.5 Exposure to gases and liquids
7 Instrument characterization[8]
7.1 General
6.4 Handling and mounting of specimens
6.5 Specimen treatments
6.5.1 General
6.5.2 Heating and cooling
6.5.3 Scraping and fracture
6.5.4 Ion bombardment for analysing thin films
6.5.5 Exposure to gases and liquids
7 Instrument characterization[8]
7.1 General
16 7.2 Instrument checks
7.2.1 System health check[9]
7.2.2 Mechanical
7.2.3 Sample holder
7.2.4 Vacuum
7.3 Instrument calibration
7.3.1 Calibration of binding energy scale
7.2 Instrument checks
7.2.1 System health check[9]
7.2.2 Mechanical
7.2.3 Sample holder
7.2.4 Vacuum
7.3 Instrument calibration
7.3.1 Calibration of binding energy scale
18 7.3.2 Intensity repeatability and intensity/energy response function (IERF)
7.3.2 Intensity repeatability and intensity/energy response function (IERF)
19 7.3.3 Linearity of intensity scale test
7.3.3 Linearity of intensity scale test
20 7.3.4 Lateral resolution
7.3.5 Depth resolution[21][22]
7.3.4 Lateral resolution
7.3.5 Depth resolution[21][22]
22 7.3.6 Charge correction
7.4 Instrument set-up
7.4.1 Optimum settings
7.3.6 Charge correction
7.4 Instrument set-up
7.4.1 Optimum settings
23 7.4.2 System configuration
8 The wide-scan spectrum
8.1 Data acquisition
8.1.1 General
8.1.2 Energy resolution
8.1.3 Energy range, step size and acquisition mode
8.1.4 Charge correction
7.4.2 System configuration
8 The wide-scan spectrum
8.1 Data acquisition
8.1.1 General
8.1.2 Energy resolution
8.1.3 Energy range, step size and acquisition mode
8.1.4 Charge correction
24 8.2 Data analysis
8.2.1 Peak identification and labelling
8.2 Data analysis
8.2.1 Peak identification and labelling
25 8.2.2 Peak intensity
8.2.3 Element-specific data
8.2.4 Assessment and utilization of peak intensities[34]
8.2.5 Assessment and utilization of background[35]
8.2.6 Assessment of wide-scan spectrum
8.2.2 Peak intensity
8.2.3 Element-specific data
8.2.4 Assessment and utilization of peak intensities[34]
8.2.5 Assessment and utilization of background[35]
8.2.6 Assessment of wide-scan spectrum
26 9 The narrow scan
9.1 General
9.2 Data acquisition
9.2.1 Instrument settings
9.2.2 Choice of region
9.3 Data analysis
9.3.1 Element identification
9.3.2 Chemical-state identification
9.3.2.1 Methods of identifying chemical state[44]
9 The narrow scan
9.1 General
9.2 Data acquisition
9.2.1 Instrument settings
9.2.2 Choice of region
9.3 Data analysis
9.3.1 Element identification
9.3.2 Chemical-state identification
9.3.2.1 Methods of identifying chemical state[44]
27 9.3.2.2 Assessment of compositional inhomogeneities in the sample[34]
9.3.2.3 Estimation and assessment of trial sample composition
9.3.2.4 Consideration of possibility of multiple compounds in sample
9.3.3 Quantification
9.3.3.1 Measurement of peak intensities[34]
9.3.2.2 Assessment of compositional inhomogeneities in the sample[34]
9.3.2.3 Estimation and assessment of trial sample composition
9.3.2.4 Consideration of possibility of multiple compounds in sample
9.3.3 Quantification
9.3.3.1 Measurement of peak intensities[34]
28 9.3.3.2 Measurement of composition for an identified phase (homogeneous sample)
9.3.3.3 Measurement of composition as a function of depth
9.3.3.2 Measurement of composition for an identified phase (homogeneous sample)
9.3.3.3 Measurement of composition as a function of depth
29 9.3.3.4 Measurement of overlayer-film thickness
9.3.3.4 Measurement of overlayer-film thickness
30 9.3.3.5 Measurement of composition as a function of lateral position on the sample
10 Test report
9.3.3.5 Measurement of composition as a function of lateral position on the sample
10 Test report
BS ISO 10810:2010
$167.15