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BS ISO 15633:2017

$102.76

Iron ores. Determination of nickel. Flame atomic absorption spectrometric method

Published By Publication Date Number of Pages
BSI 2017 22
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This document specifies a flame atomic absorption spectrometric method for the determination of the nickel mass fraction of iron ores.

This method is applicable to mass fractions of nickel between 0,001 % and 0,10 % in natural iron ores, iron ore concentrates and agglomerates including sinter products.

This method is not appropriate for referee purposes.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
8 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
9 5 Reagents
6 Apparatus
10 7 Sampling and samples
7.1 Laboratory sample
7.2 Preparation of predried test samples
11 8 Procedure
8.1 Number of determinations
8.2 Test portion
8.3 Blank test and check test
8.4 Determination
8.4.1 Decomposition of the test portion
12 8.4.2 Removal of iron
8.4.3 Treatment of the residue
8.4.4 Preparation of the calibration solutions
13 8.4.5 Adjustment of the atomic absorption spectrometer
8.4.6 Atomic absorption measurements
9 Expression of results
9.1 Calculation of nickel content
14 9.2 General treatment of results
9.2.1 Repeatability and permissible tolerance
9.2.2 Determination of analytical result
9.2.3 Between-laboratories precision
15 9.2.4 Check for trueness
16 9.2.5 Calculation of final result
9.3 Oxide factor
10 Test report
18 Annex A (normative) Flowsheet of the procedure for the acceptance of analytical values for test samples
19 Annex B (informative) Derivation of repeatability and permissible tolerance formulae
20 Annex C (informative) Precision data obtained by international analytical trial
21 Bibliography
BS ISO 15633:2017
$102.76