{"id":408647,"date":"2024-10-20T05:31:42","date_gmt":"2024-10-20T05:31:42","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-157492022\/"},"modified":"2024-10-26T10:04:48","modified_gmt":"2024-10-26T10:04:48","slug":"bs-en-157492022","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-157492022\/","title":{"rendered":"BS EN 15749:2022"},"content":{"rendered":"
This document specifies three different methods (Methods A, B and C) for the determination of sulfur present in fertilizer extracts in the form of sulfates. Method A specifies the gravimetric method. Method B specifies the method using inductively coupled plasma optical spectrometry (ICP-OES). Method C specifies the method using ion chromatography (IC).<\/p>\n
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2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 4.1 Method A: Gravimetric method 4.2 Method B: ICP-OES <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | 4.3 Method C: IC 5 Sampling and sample preparation 6 Method A \u2013 Gravimetric method 6.1 Reagents 6.2 Apparatus 6.3 Procedure 6.3.1 Sampling of the solution 6.3.2 Preparation of the precipitate <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 6.3.3 Incineration and weighing of the precipitate 6.4 Calculation and expression of the result 7 Method B \u2013 ICP-OES method 7.1 Reagents <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 7.2 Apparatus 7.3 Preparation of the extract 7.4 Procedure 7.4.1 General 7.4.2 Preparation of the test solution 7.4.3 Preparation of the blank test solution <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 7.4.4 Preparation of the calibration solutions 7.5 Determination 7.5.1 General 7.5.2 Determination by ICP-OES <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 7.6 Calculation and expression of the results 7.6.1 Calculation <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 7.6.2 Expression of the sulfur content in the sample 8 Method C \u2013 IC method 8.1 Reagents <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 8.2 Apparatus <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 8.3 Sampling and sample preparation (EN 1482-1) 8.4 Procedure 8.4.1 Preparation of the test solution 8.4.2 Preparation of the calibration solutions 8.4.2.1 Calibration by standard addition 8.4.2.2 External calibration <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 8.4.3 Determination 8.4.3.1 General 8.4.3.2 Determination by ion chromatography (IC) 8.4.3.3 Procedure 8.4.3.4 Calibration 8.4.3.5 Measurement <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 8.4.3.6 Validity check of the calibration function 8.5 Expression of the results 8.5.1 Calculation of results using standard addition technique <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | 8.5.2 Calculation of results using external calibration <\/td>\n<\/tr>\n | ||||||
19<\/td>\n | 9 Precision of methods A, B and C 9.1 Inter-laboratory tests 9.2 Repeatability 9.3 Reproducibility <\/td>\n<\/tr>\n | ||||||
21<\/td>\n | 10 Test report <\/td>\n<\/tr>\n | ||||||
22<\/td>\n | Annex A (informative)Statistical results of the inter-laboratory tests <\/td>\n<\/tr>\n | ||||||
25<\/td>\n | Annex B (informative)Statistical results of the inter-laboratory tests of VDLUFA <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | Annex C (informative)Statistical results of the inter-laboratory tests of Spanish Proficiency Testing Program <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Fertilizers. Determination of sulfates content using three different methods<\/b><\/p>\n |