{"id":60164,"date":"2024-10-17T11:19:26","date_gmt":"2024-10-17T11:19:26","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-e2838-2011\/"},"modified":"2024-10-24T17:45:25","modified_gmt":"2024-10-24T17:45:25","slug":"astm-e2838-2011","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-e2838-2011\/","title":{"rendered":"ASTM-E2838 2011"},"content":{"rendered":"

ASTM E2838-11<\/h3>\n

Historical Standard: Standard Test Method for Determination of Thiodiglycol on Wipes by Solvent Extraction Followed by Liquid Chromatography\/Tandem Mass Spectrometry (LC\/MS\/MS)<\/h4>\n
\n

ASTM E2838<\/h4>\n

Scope<\/strong><\/p>\n

1.1 This procedure details the determination of thiodiglycol (TDG), also known as 2,2\u2019<\/span>-thiobis-ethanol, on wipes with 3,3\u2019<\/span>-thiodipropanol (TDP) as the surrogate. This method is based upon solvent extraction of wipes by either sonication or a pressurized fluid extraction (PFE) technique as an alternative option. The extract is filtered, concentrated and analyzed by liquid chromatography\/tandem mass spectrometry (LC\/MS\/MS). TDG is qualitatively and quantitatively determined.<\/p>\n

1.2 Units<\/span>\u2014<\/span>The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.<\/p>\n

1.3 The Method Detection Limit (MDL) and Reporting Range for TDG are listed in Table 1.<\/p>\n

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.<\/span><\/p>\n

Keywords<\/strong><\/p>\n

chemical warfare agent; liquid chromatography; mass spectrometry; pressurized fluid extraction; single reaction monitoring; sonication; thiodiglycol; wipe<\/p>\n

ICS Code<\/strong><\/p>\n

ICS Number Code n\/a<\/p>\n

DOI:<\/strong> 10.1520\/E2838-11<\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
1<\/td>\nScope
Referenced Documents
Terminology
Summary of Test Method
TABLE 1 <\/td>\n<\/tr>\n
2<\/td>\nSignificance and Use
Interferences
Apparatus <\/td>\n<\/tr>\n
3<\/td>\nReagents and Materials
Hazards
Glassware Washing, Sampling and Preservation <\/td>\n<\/tr>\n
4<\/td>\nPreparation of LC\/MS\/MS
Calibration and Standardization
TABLE 2
TABLE 3 <\/td>\n<\/tr>\n
5<\/td>\nTABLE 4
TABLE 5 <\/td>\n<\/tr>\n
6<\/td>\nSonication Procedure
TABLE 6 <\/td>\n<\/tr>\n
7<\/td>\nPressurized Fluid Extraction Procedure (PFE) (Optional)
Calculation or Interpretation of Results
Report
TABLE 7 <\/td>\n<\/tr>\n
8<\/td>\nPrecision and Bias
Keywords
TABLE 8 <\/td>\n<\/tr>\n
9<\/td>\nTABLE 9
TABLE 10 <\/td>\n<\/tr>\n
10<\/td>\nTABLE 11 <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

E2838-11 Standard Test Method for Determination of Thiodiglycol on Wipes by Solvent Extraction Followed by Liquid Chromatography\/Tandem Mass Spectrometry (LC\/MS\/MS)<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
ASTM<\/b><\/a><\/td>\n2011<\/td>\n10<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":60165,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2637],"product_tag":[],"class_list":{"0":"post-60164","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-astm","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/60164","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/60165"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=60164"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=60164"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=60164"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}