{"id":302505,"date":"2024-10-19T20:40:04","date_gmt":"2024-10-19T20:40:04","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-103782016\/"},"modified":"2024-10-25T18:11:39","modified_gmt":"2024-10-25T18:11:39","slug":"bs-iso-103782016","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-103782016\/","title":{"rendered":"BS ISO 10378:2016"},"content":{"rendered":"
This International Standard specifies a fire assay gravimetric and flame atomic absorption spectrometric method for the determination of the mass fraction of gold and silver in copper, lead, and zinc sulfide concentrates as follows.<\/p>\n
Copper concentrates<\/p>\n
The method is applicable to the determination of mass fractions of gold from 0,5 g\/t to 300 g\/t and of mass fractions of silver from 25 g\/t to 1 500 g\/t in copper sulfide concentrates containing mass fractions of copper from 15 % to 60 %.<\/p>\n<\/li>\n
Lead concentrates<\/p>\n
The method is applicable to the determination of mass fractions of gold from 0,1 g\/t to 25 g\/t and of mass fractions of silver from 200 g\/t to 3 500 g\/t in lead sulfide concentrates containing mass fractions of lead from 10 % to 80 %.<\/p>\n<\/li>\n
Zinc concentrates<\/p>\n
The method is applicable to the determination of mass fractions of gold from 0,1 g\/t to 12 g\/t and of mass fractions of silver from 10 g\/t to 800 g\/t in zinc sulfide concentrates containing mass fractions of zinc up to 60 %.<\/p>\n<\/li>\n<\/ul>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
7<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | Introduction <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 1\tScope 2\tNormative references <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 3\tPrinciple 3.1\tGeneral 3.2\tFusion 3.3\tCupellation 3.4\tParting 3.5\tRetreatment 3.6\tCorrection for blank contamination 4\tReagents <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 5\tApparatus <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 6\tSample 6.1\tTest sample 6.2\tTest portion <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 7\tProcedure 7.1\tNumber of determinations 7.2\tTrial fusion 7.3\tBlank tests 7.4\tCharge preparation <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 7.5\tPrimary fusion <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 7.6\tCupellation 7.7\tRetreatment of residues <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 7.8\tDetermination of gold in the primary bead <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | 7.9\tDetermination of gold and silver in secondary beads and blanks, and of silver in prills <\/td>\n<\/tr>\n | ||||||
19<\/td>\n | 7.10\tDetermination of silver in the parting solution <\/td>\n<\/tr>\n | ||||||
20<\/td>\n | 8\tExpression of results 8.1\tMass fraction of gold <\/td>\n<\/tr>\n | ||||||
21<\/td>\n | 8.2\tMass fraction of silver <\/td>\n<\/tr>\n | ||||||
22<\/td>\n | 9\tPrecision 9.1\tExpression of precision <\/td>\n<\/tr>\n | ||||||
23<\/td>\n | 9.2\tMethod for obtaining the final result (see Annex\u00a0H) 9.3\tPrecision between laboratories <\/td>\n<\/tr>\n | ||||||
25<\/td>\n | 9.4\tCheck of trueness 9.4.1\tGeneral <\/td>\n<\/tr>\n | ||||||
26<\/td>\n | 9.4.2\tType of certified reference material (CRM) or reference material (RM) 10\tTest report <\/td>\n<\/tr>\n | ||||||
27<\/td>\n | Annex\u00a0A (normative) Procedure for the preparation and determination of the mass of a predried test portion <\/td>\n<\/tr>\n | ||||||
29<\/td>\n | Annex\u00a0B (normative) Trial fusion <\/td>\n<\/tr>\n | ||||||
30<\/td>\n | Annex\u00a0C (normative) Blank determination <\/td>\n<\/tr>\n | ||||||
31<\/td>\n | Annex\u00a0D (normative) Inquartation <\/td>\n<\/tr>\n | ||||||
32<\/td>\n | Annex\u00a0E (normative) Determination of vaporization loss of silver during the cupellation process <\/td>\n<\/tr>\n | ||||||
33<\/td>\n | Annex\u00a0F (normative) Sulfuric acid \u2014 Parting <\/td>\n<\/tr>\n | ||||||
35<\/td>\n | Annex\u00a0G (normative) Determination of impurities in parting solutions and washings <\/td>\n<\/tr>\n | ||||||
39<\/td>\n | Annex\u00a0H (normative) Flowsheet of the procedure for the acceptance of analytical values for test samples (see 9.2) <\/td>\n<\/tr>\n | ||||||
40<\/td>\n | Annex\u00a0I (informative) Flowsheet of the method <\/td>\n<\/tr>\n | ||||||
41<\/td>\n | Annex\u00a0J (informative) Roasting method <\/td>\n<\/tr>\n | ||||||
42<\/td>\n | Annex\u00a0K (informative) Guide to the preparation of dilutions for the determination of silver in parting solutions and residues <\/td>\n<\/tr>\n | ||||||
43<\/td>\n | Annex\u00a0L (informative) Derivation of precision equations <\/td>\n<\/tr>\n | ||||||
58<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Copper, lead and zinc sulfide concentrates. Determination of gold and silver. Fire assay gravimetric and flame atomic absorption spectrometric method<\/b><\/p>\n |