{"id":379976,"date":"2024-10-20T03:04:52","date_gmt":"2024-10-20T03:04:52","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-cen-iso-ts-221152021\/"},"modified":"2024-10-26T05:33:42","modified_gmt":"2024-10-26T05:33:42","slug":"bsi-pd-cen-iso-ts-221152021","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-cen-iso-ts-221152021\/","title":{"rendered":"BSI PD CEN ISO\/TS 22115:2021"},"content":{"rendered":"
This method is suitable for the semi-quantitative analysis of oils, fats and oil\/fat-related samples (deodistillates). Screening of oils, fats and oil\/fat-related samples to obtain main (e.g. TAGs) and minor component (e.g. sterols, sterol esters, tocopherols, squalene, wax esters, fatty alcohols, and glycerol) information in one single analysis. For a truly quantitative analysis of pre-identified compound classes specific methods are more appropriate. Beside the (semi-)quantitative determination of the oil\/fat composition mentioned above, the method can also be used as a useful qualitative screening tool for the relative comparison of sample compositions.<\/p>\n
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2<\/td>\n | National foreword <\/td>\n<\/tr>\n | ||||||
4<\/td>\n | European foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 5 Reagents <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | 6 Apparatus <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 6.8 Ultrasonic bath. 6.9 Nitrogen evaporator. 7 Sample 7.1 Sampling 7.2 Preparation of test sample 8 Procedure 8.1 Preparation of the internal standard, tridecanoylglycerol (5.2.5), c = 20 mg\/ml 8.2 Preparation of the individual standard solutions for determination of response factors <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 8.3 Silylation of the standards 8.4 Preparation of the sample 8.5 Sample solution 8.6 Silylation of the sample 8.7 Gas chromatography <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 8.8 Peak identification and integration 9 Result of the determination 9.1 Calculation of the response factor <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 9.2 Quantitative determination 10 Precision of the method 10.1 Interlaboratory test <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 10.2 Repeatability 10.3 Reproducibility 11 Test report <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | Annex A (informative) Typical chromatograms <\/td>\n<\/tr>\n | ||||||
24<\/td>\n | Annex B (informative) Results of an interlaboratory test <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Animal and vegetable fats and oils. Separation of lipid classes by capillary gas chromatography (fingerprint method)<\/b><\/p>\n |