{"id":402784,"date":"2024-10-20T05:02:54","date_gmt":"2024-10-20T05:02:54","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-iso-213632022\/"},"modified":"2024-10-26T08:59:06","modified_gmt":"2024-10-26T08:59:06","slug":"bs-en-iso-213632022","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-iso-213632022\/","title":{"rendered":"BS EN ISO 21363:2022"},"content":{"rendered":"
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
5<\/td>\n | European foreword Endorsement notice <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | Introduction <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 1 Scope 2 Normative references 3 Terms, definitions and symbols 3.1 Core terms \u2014 Particles <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 3.2 Core terms \u2014 Image capture and analysis <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 3.3 Core terms \u2014 Statistical symbols and definitions <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 3.4 Core terms \u2014 Measurands <\/td>\n<\/tr>\n | ||||||
20<\/td>\n | 3.5 Core terms \u2014 Metrology <\/td>\n<\/tr>\n | ||||||
23<\/td>\n | 3.6 Core terms \u2014 Transmission electron microscopy <\/td>\n<\/tr>\n | ||||||
24<\/td>\n | 3.7 Statistical symbols, measurands and descriptors 3.7.1 Statistical symbols 3.7.2 Measurands and descriptors <\/td>\n<\/tr>\n | ||||||
25<\/td>\n | 4 Stakeholder needs for TEM measurement procedures <\/td>\n<\/tr>\n | ||||||
26<\/td>\n | 5 Sample preparation 5.1 General <\/td>\n<\/tr>\n | ||||||
27<\/td>\n | 5.2 Sample sources 5.3 Use a representative sample 5.3.1 General 5.3.2 Powder samples 5.3.3 Nanoparticle dispersions in liquids <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | 5.4 Minimize particle agglomeration in the sample dispersion 5.5 Selection of the mounting support 6 Instrument factors 6.1 Instrument set-up <\/td>\n<\/tr>\n | ||||||
29<\/td>\n | 6.2 Calibration 6.2.1 General 6.2.2 Calibration standards 6.2.3 General calibration procedure <\/td>\n<\/tr>\n | ||||||
31<\/td>\n | 6.3 Setting TEM operating conditions for calibration <\/td>\n<\/tr>\n | ||||||
32<\/td>\n | 7 Image capture 7.1 General 7.2 Setting a suitable operating magnification <\/td>\n<\/tr>\n | ||||||
33<\/td>\n | 7.3 Minimum particle area 7.4 Number of particles to count for particle size and shape distributions <\/td>\n<\/tr>\n | ||||||
34<\/td>\n | 7.5 Uniform background 7.6 Measurement procedure 7.6.1 General <\/td>\n<\/tr>\n | ||||||
35<\/td>\n | 7.6.2 Developing a test sample 7.6.3 Effects of magnification 7.6.4 Frames (micrographs) 7.7 Revision of image capture protocols 8 Particle analysis 8.1 General 8.2 Individual particle analysis <\/td>\n<\/tr>\n | ||||||
36<\/td>\n | 8.3 Automated particle analysis 8.4 Example \u2014 Automated particle analysis procedure <\/td>\n<\/tr>\n | ||||||
37<\/td>\n | 9 Data analysis 9.1 General 9.2 Raw data triage \u2014 Detecting touching particles, unselected particles, artefacts and contaminants <\/td>\n<\/tr>\n | ||||||
38<\/td>\n | 9.3 Data quality assessment \u2014 Repeatability, intermediate precision and reproducibility <\/td>\n<\/tr>\n | ||||||
40<\/td>\n | 9.4 Fitting distributions to data <\/td>\n<\/tr>\n | ||||||
41<\/td>\n | 9.5 \u200bAssessing measurement uncertainty for samples under repeatability, intermediate precision or reproducibility conditions 9.5.1 Grand statistics for fitted parameters \u2014 Three or more datasets 9.5.2 Measurement uncertainty of fitted parameters <\/td>\n<\/tr>\n | ||||||
42<\/td>\n | 9.5.3 Example \u2014 Measurement uncertainty for a size descriptor 9.6 Bivariate analysis <\/td>\n<\/tr>\n | ||||||
43<\/td>\n | 10 Reporting <\/td>\n<\/tr>\n | ||||||
46<\/td>\n | Annex A (informative) Case studies overview <\/td>\n<\/tr>\n | ||||||
48<\/td>\n | Annex B (informative) Discrete spheroidal nanoparticles <\/td>\n<\/tr>\n | ||||||
51<\/td>\n | Annex C (informative) Size mixture <\/td>\n<\/tr>\n | ||||||
63<\/td>\n | Annex D (informative) Shape mixture <\/td>\n<\/tr>\n | ||||||
68<\/td>\n | Annex E (informative) Amorphous aggregates <\/td>\n<\/tr>\n | ||||||
72<\/td>\n | Annex F (informative) Nanocrystalline aggregates <\/td>\n<\/tr>\n | ||||||
76<\/td>\n | Annex G (informative) Nanofibres with irregular cross-sections <\/td>\n<\/tr>\n | ||||||
83<\/td>\n | Annex H (informative) Nanoparticles with specific crystal habits <\/td>\n<\/tr>\n | ||||||
90<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Nanotechnologies. Measurements of particle size and shape distributions by transmission electron microscopy<\/b><\/p>\n |